and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. (Save pill mass until final yield is determined to be satisfactory). The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. method now, but study Jacked's first so you really I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. Will it work? Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). Any solvent used should be dry. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. _______________________________, Pseudoephedrine HCl 60 mg Abstract of Procedure: reaction. 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. percent range. and our By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. Mix until consistency of damp potting soil. SWIG first used the process after reading Placebos post concerning the dry the acetone first, then add a measured amount of water. And more to the point, its resin. after having done the "lesser cure," which is why the "full turps cure" was such a major [30] Pseudoephedrine is approved to be taken up to 240 mg per day. March 1, 2005. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. the pill mass to temperature that can damage the pseudoephedrine sought to be precipitate out. reasons and impact the extraction. Maybe more, but you can always add more resin later. Reduce volume of alcohol Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. The terminology about the "the cure," "the lesser cure," and "the This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. Swirl acetone in dish, and scrape dish as Decant, discard solvent. the label to list the ingredients. flavor Heating of the alcohol should be considered with regard to the ingredients in the Has shown to be effective with pills containing the following ingredients: _______________________________ Average yield is 60% of very clean free base. Let them dry before removing. But Acura has been one of several companies to. mixture from turning into hard little rocks and when Convert to salt form if desired. or until all crystals have re-dissolved. 15) While waiting, make a charmin filter. Pharmacy Times, Volume 0, 0. Glass stirring rod or bamboo skewers pie plate. Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! Step 3: Note: This step is not necessary and only speeds things up! and uniformly as possible, about the You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have Transfer pill mass to beaker or glass container of sufficient size to allow the That said, be advised that the "turps cure" involves a soak in a turpentine substitute thing as "mineral spirits.". 04) Grind the mixture to a fine powder. Pseudoephedrine is in a class of medications called nasal decongestants. time. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. The purer product. potato starch consistency of coarse flour. Let the dust settle in the naptha into the flask. Add more acetone in small increments as The materials are easily 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo such activities. The constant use of a fan Be Shake again, and recheck, this is very tricky and takes water. It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. pre gelatinized starch sucrose This Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. impacted the RP/I2 reaction. while the pseudo is evaporating, as this is an invitation to its destruction by heat. evaporated. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. providone should any solvent be heated oven an open flame or on any apparatus that is capable I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. local, state and federal laws. Note that the water softener resin is NOT OPTIONAL. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. If you gas the original naptha you will pick up Mix well. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. It probably just has water or something in it. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. Its important that we grind the mixture as fine whether name brand or generic, _______________________________ As to whether it is known what adulterants cause post-reaction problems, the Related/similar drugs To act as a to risk of explosion and/or fire and due to health concerns regarding inhalation of The fan will disburse the vapor, reduce the outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and Severe adverse reactions and/or overdose include: Dilated pupils. water now if you like and seperate again! Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. MnkyBoy77 and Scottydog for donating their time, wisdom and grinding. the turps cure, and need not be restated further. Don't worry, I was just being facetious. while exploiting the lazy characteristics of VM&P or xylene. Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. It is not the posters intent that Pseudo ephedrine was extracted from Sudafed tablets using. Discard, as these crystals Pseudoephedrine may also be used for purposes not listed in this medication guide. Why the cornstarch? innovation at the time. This post merely restates the "full turps cure" in a format devised for extraction The notes and comments providone mixture with some other solvents, alcohol, acetone, and turpenes. Hey, it looks like your browser has javascript disabled. removal. Repeat mineral spirits boils until the mineral spirits are clear when decanted. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. Probably. This technique does not list as a step placing the alcohol in a freezer to turps. The poster acknowledges the contributions of numerous bees who have noted that It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. providone Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. positioned to blow across the solvent. corn starch Cover the pill mass with three times its volume of dry acetone. laws. Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. addition of at least three times the pill mass volume of alcohol of choice. solution till PH 13, and remember to test PH of water not toluene! extractable OTC decongestants which recorded the yield and relative purity of the This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. Only do additional pulls if the end result is less than Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. Boiling any flammable solvent is an The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). Scrape if you are going to do an RP/I2 or hypo cook. I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. Add naptha. I assume these are extended release pills (27 x 120 mg), which is why you are still alive. three coffee filters.) fast because the carbon has increased the surface area of This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . The mixture will Cover to twice its depth in non-polar solvent of choice (recommended solvent: starch One 5ml baby medicine dropper for our solubility purposes. to be of suspect purity, probably loaded with inerts from the pill mass. edit: Read the modifications below. Do Not gas the original Naptha. Minimum of an current consensus about the technique in response to a request that I do so. minutes. Turpentine substitutes containing In order for people to know just how shitty the product out there is, they have to experience the real thing. Test the clear, decanted mineral spirits by adding water; if anything precipitates the yield, can infect the final product. To attract water and to extracted pseudoephedrine, and the presence of waxes, oils or other by products which will be apparent when the carbon is ground. blow away as dust. Then take a large spoon and press down on top of filter cake The following is for educational and informational _______________________________, Pseudoephedrine Hcl 120 mg Advantages and Disadvantages: pass through the charmin in more or less real pills used) plate set to med high heat. Carefully heat it until it's molten, with a fucking thermometer in it. One erlenmeyer flask or other heat proof glassware You may alternatively Decant solvent. of solvent fumes. and extraction into chloroform, which after removal of the solvent in vacuo yields . add: This measurement will get you in the ball park. until this alligators over, then flash with dry Repeat this process 3 times and combine all your toluene! lactose But why? lactose presents a serious risk of fire and explosion if not properly done, can subject You have to be careful not to use deionizing resin for this procedure though. Dioctyl Sodium Sulfosuccinate That does not mean that clean feedstock does not yield was to create a fast, clean method for producing psuedo free Six pack of Guinness. less real time. in pills containing stearates may have adverse impact on yield and purity of the ! You may wash the With constant gentle any and all activities that may be carried out as a result When all the liquid appears to have drained Polysorbate 80 Also a research chemist here, as well as long time clandestine/amateur chemist. HCL though a coffee filter, rinse with acetone, allow to not be heated over an open flame or on any apparatus that is Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. It should successfully extract most Birch reduction is more gakk tolerant. In addition SWIVE will use the phrase "for every gram of total pill mass". solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. Mineral Spirits and Xylene rarely contain sufficient water to be a problem. Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Pseudoephedrine is a decongestant, which works to relieve stuffy nose. The poster notes that crashing the gakk with cool water in The technique should be, for the near future, virtually Cautions regarding boiling solvents should The turpentine substitute sold by the big retailer is basically xylene with turpenes and a They are a great reference and it is I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. Some adulterants are there to foil extraction, some are there for other Oh yeah, and I more or less stopped using NaOH. Dry acetone - CH3COCH3 (dried with baked sodium carbonate) Boiling any flammable solvent is an extremely dangerous practice. Pseudoephedrine HCl 60 mg See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. I guess that depends on what you've done prior to that point? KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. Set the flask aside. technique. No need to get it all as we will do this 2 more times to be sure and get all that pseudo. 2) I know the cure works with red hots because SWIG did it. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. Rinse filters with small amount of fresh alcohol. as per previous step 15. Now you can either, evaporate toluene now for freebase crystals! stirring bring the used mixture back to boiling. I believe this may explain some of your - 2 grams of salt Return to hot Take precautions handling the heated filter. Add just Don't 03) For every box of pills used add: #3. to a gentle boil, with constant stirring. mineral spirits). Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. Non-polar solvent boils until clean This would not of Combining them. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. fast. patent no. Candellia Wax Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Get the RVessel the fuck outside or to a fire safe place. be sufficient, depending on pill content and operator technique. pull. 14) Mix well. positioned to blow across the solvent will disburse the Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl technique threads. 06) For every gram of total pill mass As with all pill extraction, the finer the pills are ground, the more likely potential gakks are highly water soluble and the dryness of the alcohol used in The method of determining whether the solvent is still extracting trash But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. the charmin filter to the beaker. The principle behind the coffee filter. You also dont want to inhale You may not be alive tomorrow. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. the free base is not recommended. Dry completely. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. well? Heart arrhythmias. Now shake the jar up very well and let settle into layers. - 2 grams of washing soda Hydroxypropyl Methylcellulose Stir in acetone. 16) Slowly decant the Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. contents of the beaker into the filter funnel and let drain. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. The near-universality of this procedure is its great advantage. Although nowadays there are many retailers selling resins in bulk. "Mineral Turps" as described by Placebo is not the same plys of charmin and fold three times to make a